This contributed volume provides a comprehensive overview of how artificial intelligence (AI) and machine learning (ML) are transforming experimental research in nanomaterials. It covers foundational AI concepts, data acquisition and preprocessing tailored to nanomaterials and explores AI-enhanced synthesis and characterization techniques. The volume discusses applications in catalysis, environmental remediation, energy storage, and sensor technologies, emphasizing green synthesis and high-performance materials. It concludes with future directions, including responsible AI practices, policy frameworks, and educational strategies. Designed for graduate students, academic researchers, and R&D professionals in materials science, chemistry, physics, nanotechnology, and engineering, as well as policymakers and educators, this book aims to illuminate how AI can revolutionize nanomaterials research for energy, environmental, and biomedical applications.

Dr. Ramachandra Naik is a distinguished Associate Professor of Physics at New Horizon College of Engineering, Bangalore, India, recognized among the World’s Top 2% Scientists (Stanford University & Elsevier). A Fellow of the Royal Society of Chemistry (FRSC), he brings over 14 years of research and teaching experience in nanoscience and energy materials. Dr. Naik has authored six books, edited two volumes, and published 84 research/review articles, conference papers, and book chapters in leading international journals. His research focuses on the green synthesis of multifunctional inorganic metal oxide-based nanomaterials for advanced energy storage, catalysis, and sensor applications.

Dr. H. P. Nagaswarupa is a Professor in the Department of Studies in Chemistry at Davangere University, India, and a Fellow of the Royal Society of Chemistry (FRSC). With an academic career spanning over two decades, he has published more than 180 papers in reputed national and international journals. His prolific research encompasses Nanoscience & Technology, Materials Science, and Corrosion Science, and he is widely recognized for his contributions to the development of functional nanomaterials and surface-engineered coatings.

Dr. Ganesh Koyyada is an Assistant Professor at Yeungnam University, South Korea, where he has served since 2017. He earned his Ph.D. in Chemical Science from the Indian Institute of Chemical Technology (IICT), Hyderabad, India. His research focuses on photocatalytic and photoelectrochemical water splitting, the design and synthesis of porous materials, non-enzymatic biosensors, and dye-sensitized solar cells. Dr. Koyyada has received several honors, including the Senior Research Fellowship from the Council of Scientific and Industrial Research (CSIR), Government of India, and serves as a guest editor for special issues in reputed international journals.